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mcw (63) in science • 7 years ago (edited)

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7 years ago by mcw (63)

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mountain.phil28 (59) · 7 years ago

Hahaha so cool, that you also had to do this kind of stuff! :)

I see, you are busy in the lab. It is the same for me, thus I hardly find time to prepare in-depth posts for STEEMIT. But for chemists like us one thing is clear: Lab work first. :)

Right now I am also experimenting to find novel ways of performing quite distinct conversions. So again back to a lot of tiny experiments screening for discrete convenient parameters. Yeay! Haha, but still way better than losing your precious substrates. :)

Thanks for the mentioning, good luck in the lab and keep posting such cool stuff!
Best,
mountain.phil28

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mcw (63) · 7 years ago

So true T.T Lab work first
But it only works for stuff with large separation on TLC and non water-sensitive experiments.
Sometimes I am not confident enough to tell that failing a miligram scale reaction is just because the product is so little, or i stuff like moisture ruined my reaction /.\

Yeah!!!! it is really coherent when I saw your pipette column post!!!!!

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mountain.phil28 (59) · 7 years ago

Yop thats true. Luckily my recently produced intermediats are not that sensitive towards humidity, but funnily they degrade in CDCl3, thus I have to be rather fast in measuring my NMRs. xD

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mcw (63) · 7 years ago

haha, chloroform is quite tricky. I was having a silylenol ether decomposed in a old bottle of chloroform(but not a new one) due to the decomposed HCl, which spend me a few whole day to figure that out 🙈