I stumbled on this write-up. It is nice and will be helpful except that the topic should have read "the size of crystallite (crystallite size)" as you can't use XRD to determine nanoparticle size.
XRD (Crystallite size)
TEM (Nanoparticle size)
SEM (Grain size).
RE: A guide to determine the size of nanoparticles using Debye Scherrer equation
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A guide to determine the size of nanoparticles using Debye Scherrer equation